3-Chloro-4-methanesulfonylaniline → 3-Hydroxymethyl-4-(methylsulfonyl)phenylhydrazine hydrochloride

HRID 2086699Notes

Reaction equation

HRID 2086699 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:7]=[CH:8][C:9]=1[S:10]([CH3:13])(=[O:12])=[O:11])[NH2:6].[Cl:14]C1C=C(C=CC=1S(C)(=O)=O)[NH2:18]>>[ClH:14].[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([NH:6][NH2:18])[CH:7]=[CH:8][C:9]=1[S:10]([CH3:13])(=[O:12])=[O:11]

Participants

3

Reactant 2

HCID 108459213-Chloro-4-methanesulfonylanilineHCID 223166243-Hydroxymethyl-4-(methylsulfonyl)aniline

Product 1

HCID 223167563-Hydroxymethyl-4-(methylsulfonyl)phenylhydrazine hydrochloride

Procedure

The title compound was prepared according to the procedure of step1 of Example 155 using 3-hydroxymethyl-4-(methylsulfonyl)aniline from step3 instead of 3-chloro-4-(methylsulfonyl)aniline.

Sources & evidence

ORD record
ord-824616f7c1c14d3d8a5060f38bc503e5
Source dataset
uspto-grants-2004_04
Patent number
US06727238B2

Reaction notes

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