m-Aminoacetanilide → HCID 15296999, compound

Participants

Reaction Steps

A mixture of 2-chloro-3-nitropyridine (6.12 g), 3′-aminoacetanilide (5.80 g) and potassium carbonate (5.34 g) in toluene (50 ml) was refluxed for 5 hours. The mixture was cooled, and the solids were collected and washed with water, ethanol and isopropyl ether successively to give 2-(3-acetamidophenyl)amino-3-nitropyridine (5.88 g) as an orange solid.

Provenance & Evidence