HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15372233, compound → HCID 22724524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15372233 | HCID 15372233 | — |
| Reactant | HCID 22724346 | HCID 22724346 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22724524 | HCID 22724524 | 70.6% |
Reaction Steps
A mixtue of 2-[3-acetylamino-5-methoxycarbonylphenylamino]-3-aminopyridine (1.07 g) and 3-(3-pyridyl)pyruvic acid (0.65 g) in methanol (15 ml) was stirred under reflux for 5 hours. The precipitate was collected and washed with methanol to give 4-(3-acetylamino-5-methoxycarbonylphenyl)-2-(3-pyridylmethyl)-3-oxo-3,4-dihydropyrido[2,3-b]pyrazine (1.08 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727245B2 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-cf35ab6d487248be9d6f7418be501769 |
| Source note | uspto-grants-2004_04 |