2-(Methylsulfonyl)ethanamine → HCID 9851149, compound

Participants

Reaction Steps

Prepared according to Procedure D from 5-(4-{3-methoxy4-(3-fluorobenzyloxy)anilino}-6-quinazolinyl)-furan-2-carbaldehyde (0.6 equiv) and 2-methanesulphonyl-ethylamine (1 equiv). 1H NMR 400 MHz (DMSO-d6) 9.22 (s,1H); 8.78 (s,1H); 8.31 (d,1H); 7.88 (d,1H); 7.50-7.08 (m,8H); 6.84 (d,1H); 5.13 (s,2H); 4.42 (s,2H); 3.80 (s,3H); 3.60 (m,2H); 3.40 (m, 2H, obscured by water peak); 3.10 (s,3H); MS m/z 577 (M+1).

Provenance & Evidence