2-[(4-Chlorophenyl)sulfanyl]thiophene-3-carbaldehyde → HCID 22048628, compound

HRID 2087382Notes

Reaction equation

HRID 2087382 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[S:10][CH:11]=[CH:12][C:13]=2[CH:14]=O)=[CH:4][CH:3]=1.[CH3:16][CH:17]([CH3:33])[C:18]([NH:20][C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([CH:27]2[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]2)[CH:22]=1)=[O:19]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([S:8][C:9]2[S:10][CH:11]=[CH:12][C:13]=2[CH2:14][N:30]2[CH2:31][CH2:32][CH:27]([C:23]3[CH:22]=[C:21]([NH:20][C:18](=[O:19])[CH:17]([CH3:16])[CH3:33])[CH:26]=[CH:25][CH:24]=3)[CH2:28][CH2:29]2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 27358102-[(4-Chlorophenyl)sulfanyl]thiophene-3-carbaldehydeHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22048628HCID 22048628, compound

Procedure

Prepared by Procedure F and Scheme R using 2-[(4- chlorophenyl)sulfanyl]-3-thiophenecarbaldehyde and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 485.0 (M+H)+.

Workup

  1. customPrepared by Procedure F and Scheme R

Sources & evidence

ORD record
ord-e1b3179443a24538981313d485d68bba
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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