1,1'-(4-Chlorobutylidene)bis(4-fluorobenzene) → HCID 22048651, compound

HRID 2087429Notes

Reaction equation

HRID 2087429 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH:5]([C:13]1[CH:18]=[CH:17][C:16]([F:19])=[CH:15][CH:14]=1)[C:6]1[CH:11]=[CH:10][C:9]([F:12])=[CH:8][CH:7]=1.[CH3:20][CH:21]([CH3:42])[C:22]([NH:24][C:25]1[CH:30]=[CH:29][C:28]([O:31][C:32]([F:35])([F:34])[F:33])=[CH:27][C:26]=1[CH:36]1[CH2:41][CH2:40][NH:39][CH2:38][CH2:37]1)=[O:23]>>[F:12][C:9]1[CH:10]=[CH:11][C:6]([CH:5]([C:13]2[CH:18]=[CH:17][C:16]([F:19])=[CH:15][CH:14]=2)[CH2:4][CH2:3][CH2:2][N:39]2[CH2:40][CH2:41][CH:36]([C:26]3[CH:27]=[C:28]([O:31][C:32]([F:35])([F:34])[F:33])[CH:29]=[CH:30][C:25]=3[NH:24][C:22](=[O:23])[CH:21]([CH3:20])[CH3:42])[CH2:37][CH2:38]2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 768201,1'-(4-Chlorobutylidene)bis(4-fluorobenzene)HCID 22049165HCID 22049165, compound

Product 1

HCID 22048651HCID 22048651, compound

Procedure

Prepared by Procedure G and Scheme AI using 1-[4-chloro-1-(4-fluorophenyl)butyl]-4-fluorobenzene and 2-methyl-N-[2-(4-piperidinyl)-4-(trifluoromethoxy)phenyl]propanamide: ESMS m/e: 574.8 (M+H)+.

Workup

  1. customPrepared by Procedure G and Scheme AI

Sources & evidence

ORD record
ord-9b8de979347c478c815ad653662aa502
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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