(2R)-3-chloro-2-methyl-1-propanol → HCID 69658006, compound

HRID 2087436Notes

Reaction equation

HRID 2087436 reaction equation
Cl[CH2:2][C@H:3]([CH3:6])[CH2:4][OH:5].[CH3:7][CH:8]([CH3:24])[C:9]([NH:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]2[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]2)[CH:13]=1)=[O:10]>>[OH:5][CH2:4][C@@H:3]([CH3:6])[CH2:2][N:21]1[CH2:22][CH2:23][CH:18]([C:14]2[CH:13]=[C:12]([NH:11][C:9](=[O:10])[CH:8]([CH3:7])[CH3:24])[CH:17]=[CH:16][CH:15]=2)[CH2:19][CH2:20]1

Participants

3

Reactant 2

HCID 10080353(2R)-3-chloro-2-methyl-1-propanolHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 69658006HCID 69658006, compound

Procedure

Prepared by Procedure G and Scheme B1 using (2R)-3-chloro-2-methyl-1-propanol and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 319.2 (M+H)+.

Workup

  1. customPrepared by Procedure G and Scheme B1

Sources & evidence

ORD record
ord-220a94b1d5da4d25a5176598f3238801
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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