3,4-Dimethoxyphenol → HCID 58651326, compound

HRID 2087528Notes

Reaction equation

HRID 2087528 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([OH:11])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].O[C@H:13]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[CH2:14][N:15]1[CH2:20][CH2:19][CH:18]([C:21]2[CH:22]=[C:23]([NH:27][C:28](=[O:32])[CH:29]([CH3:31])[CH3:30])[CH:24]=[CH:25][CH:26]=2)[CH2:17][CH2:16]1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:6]=[CH:7][C:8]=1[O:9][CH3:10])[O:11][C@@H:13]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[CH2:14][N:15]1[CH2:20][CH2:19][CH:18]([C:21]2[CH:22]=[C:23]([NH:27][C:28](=[O:32])[CH:29]([CH3:31])[CH3:30])[CH:24]=[CH:25][CH:26]=2)[CH2:17][CH2:16]1

Participants

3

Reactant 2

HCID 162513,4-DimethoxyphenolHCID 69523630HCID 69523630, compound

Product 1

HCID 58651326HCID 58651326, compound

Procedure

Prepared by Procedure B and Scheme B1 using 3,4-dimethoxyphenol and N-(3-{1-[(2R)-2-hydroxy-2-phenylethyl]-4-piperidinyl}phenyl)-2-methylpropanamide: ESMS m/e: 503.2 (M+H)+.

Workup

  1. customPrepared by Procedure B and Scheme B1

Sources & evidence

ORD record
ord-6f9c4240a58648249446fef077ed1da4
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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