2-(3-Bromopropyl)-5,5-dimethyl-1,3-dioxane → HCID 22049621, compound

HRID 2087567Notes

Reaction equation

HRID 2087567 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH:5]1[O:10][CH2:9][C:8]([CH3:12])([CH3:11])[CH2:7][O:6]1.[CH3:13][CH:14]([CH3:30])[C:15]([NH:17][C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH:24]2[CH2:29][CH2:28][NH:27][CH2:26][CH2:25]2)[CH:19]=1)=[O:16]>>[CH3:11][C:8]1([CH3:12])[CH2:9][O:10][CH:5]([CH2:4][CH2:3][CH2:2][N:27]2[CH2:28][CH2:29][CH:24]([C:20]3[CH:19]=[C:18]([NH:17][C:15](=[O:16])[CH:14]([CH3:13])[CH3:30])[CH:23]=[CH:22][CH:21]=3)[CH2:25][CH2:26]2)[O:6][CH2:7]1

Participants

3

Reactant 2

HCID 35285702-(3-Bromopropyl)-5,5-dimethyl-1,3-dioxaneHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22049621HCID 22049621, compound

Procedure

Prepared by Procedure G and Scheme B1 using 2-(3-bromopropyl)-5,5-dimethyl-1,3-dioxane and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 403.2 (M+H)+.

Workup

  1. customPrepared by Procedure G and Scheme B1

Sources & evidence

ORD record
ord-6b7b0bd2c32c4ed6b633147f7c93ac78
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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