Hydrazine, 1-naphthalenyl-, hydrochloride (1:1) → HCID 22049355, compound

HRID 2087591Notes

Reaction equation

HRID 2087591 reaction equation
[CH3:1][CH:2]([CH3:32])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:17][CH2:16][N:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][C:24](=O)[C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:14][CH2:13]2)[CH:7]=1)=[O:4].Cl.[C:34]1([NH:44]N)[C:43]2[C:38](=[CH:39][CH:40]=[CH:41][CH:42]=2)[CH:37]=[CH:36][CH:35]=1>>[CH3:1][CH:2]([CH3:32])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:17][CH2:16][N:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][C:23]3[C:35]4[C:34](=[C:43]5[CH:42]=[CH:41][CH:40]=[CH:39][C:38]5=[CH:37][CH:36]=4)[NH:44][C:24]=3[C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:14][CH2:13]2)[CH:7]=1)=[O:4]

Participants

3

Reactant 2

HCID 519949Hydrazine, 1-naphthalenyl-, hydrochloride (1:1)HCID 22048966HCID 22048966, compound

Product 1

HCID 22049355HCID 22049355, compound

Procedure

Prepared by Procedure E and Scheme M using 2-methyl-N-{3-[1-(7-oxo-7-phenylheptyl)-4-piperidinyl]phenyl}propanamide and 1-(1-naphthyl)hydrazine hydrochloride: ESMS m/e: 558.2 (M+H)+.

Workup

  1. customPrepared by Procedure E and Scheme M

Sources & evidence

ORD record
ord-a5898e106cb6457889f00bf6470dcf71
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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