1-Chloro-3-iodobenzene → 6-Chloro-1-(3-chlorophenyl)-1H-indole

HRID 2087625Notes

Reaction equation

HRID 2087625 reaction equation
[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]=[CH:7][NH:8]2)=[CH:4][CH:3]=1.[Cl:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14](I)[CH:13]=1>>[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]=[CH:7][N:8]2[C:14]2[CH:15]=[CH:16][CH:17]=[C:12]([Cl:11])[CH:13]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 122691-Chloro-3-iodobenzeneHCID 871116-Chloroindole

Product 1

HCID 220491886-Chloro-1-(3-chlorophenyl)-1H-indole

Procedure

Prepared by Procedure C and Scheme O using 6-chloro-1H-indole and 1-chloro-3-iodobenzene: ESMS m/e: 261.9 (M+H)+.

Workup

  1. customPrepared by Procedure C and Scheme O

Sources & evidence

ORD record
ord-e56e9c276edc4c59818854f46f19a356
Source dataset
uspto-grants-2004_04
Patent number
US06727264B1

Reaction notes

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