Hydrochloric Acid → HCID 22048825, compound

Participants

Reaction Steps

Prepared by Procedure A and Scheme AN using 4-chlorophenol and N-(3-{1-[5-(4-chlorophenyl)-5-hydroxypentyl]-4-piperidinyl}phenyl)-2-methylpropanamide: 1H NMR (400 MHz, CDCl3), HCl salt δ 7.86 (s, br, 1H), 7.62-6.72 (m, 12H), 5.12-5.02 (m, 1H), 3.68-3.52 (m, br, 2H), 3.02-2.82 (br, 2H), 2.82-2.56 (m, br, 4H), 2.56-2.40 (m, br, 2H), 2.06-1.80 (m, br, 6H), 1.64-1.40 (m, br, 2H), 1.25 (d, 6H, J=6.8 Hz). Anal. Calc. for C32H39Cl3N2O2.1.3MeOH: C, 63.25; H, 7.07; N, 4.42; Found: C, 63.41; H, 6.99; N, 4.17. ESMS m/e: 553.0 (M+H)+.

Provenance & Evidence