HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22048732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | HCID 22049297 | HCID 22049297 | — |
| Product | HCID 22048732 | HCID 22048732 | — |
Reaction Steps
Prepared by Procedure A and Scheme AN using 4-chlorophenol and N-{3-[1-(5-hydroxy-5-phenylpentyl)-4-piperidinyl]phenyl}-2-methylpropanamide: 1H NMR (400 MHz, CDCl3), HCl salt δ 7.72-6.72 (m, 13H), 5.12-5.04 (m, 1H), 3.66-3.52 (m, br, 2H), 3.01-2.83 (br, 2H), 2.68-2.62 (m, br, 2H), 2.62-2.48 (m, br, 4H), 2.04-1.82 (m, br, 6H), 1.62-1.40 (m, br, 2H), 1.25 (d, 6H, J=7.2 Hz); ESMS m/e: 519.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06727264B1 |
| Source dataset | uspto-grants-2004_04 |
| ORD ID | ord-df5068f385c444979c04e840c001f9d0 |
| Source note | uspto-grants-2004_04 |