HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phthaloylglycine → 2H-Isoindole-2-acetyl chloride, 1,3-dihydro-1,3-dioxo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phthaloylglycine | HCID 20825 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2H-Isoindole-2-acetyl chloride, 1,3-dihydro-1,3-dioxo- | HCID 81242 | — |
Reaction Steps
In the (G2a) step, 2 mol of thionylchloride (SOCl2) was added to the compound 1a to produce 2-(1,3-dioxoisoindolin-2-yl)acetic chloride (compound 2a) and the unreacted thionylchloride (SOCl2) was recovered by using an aspirator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08435480B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-5b13de9945bb428ebfd13df5ae26d016 |
| Source note | uspto-grants-2013_05 |