HCID 59703438, compound → HCID 59703428, compound

HRID 2088481Notes

Reaction equation

HRID 2088481 reaction equation
[F:1][CH:2]([F:22])[O:3][C:4]1[CH:12]=[CH:11][C:10]([B:13]2[O:17][C:16]([CH3:19])([CH3:18])[C:15]([CH3:21])([CH3:20])[O:14]2)=[CH:9][C:5]=1[C:6]([NH2:8])=[O:7].Br[C:24]1C=CC(OC(F)F)=C(C=1)C(NC)=O>>[F:22][CH:2]([F:1])[O:3][C:4]1[CH:12]=[CH:11][C:10]([B:13]2[O:17][C:16]([CH3:18])([CH3:19])[C:15]([CH3:21])([CH3:20])[O:14]2)=[CH:9][C:5]=1[C:6]([NH:8][CH3:24])=[O:7]

Participants

3

Reactant 2

HCID 59703438HCID 59703438, compoundHCID 59703486HCID 59703486, compound

Product 1

HCID 59703428HCID 59703428, compound

Procedure

2-Difluoromethoxy-N-methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide was prepared in a similar way as 2-Difluoromethoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide using 5-bromo-2-difluoromethoxy-N-methyl-benzamide as the starting material.

Sources & evidence

ORD record
ord-b7d032ef33be45cebdf5cf2b6e6cfe0a
Source dataset
uspto-grants-2013_05
Patent number
US08435985B2

Reaction notes

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