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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2088737Generated: November 4, 2026

Hexane isopropanol diethylamine → HCID 58289958, compound

https://huagongshe.com/reaction/2088737

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHexane isopropanol diethylamineHCID 21973129—
ReactantHCID 67224036HCID 67224036—
ProductHCID 58289958HCID 58289958—
ProductHCID 58290004HCID 58290004—

Reaction Steps

7-[(Dimethylamino)methyl]-5,6,7,8-tetrahydronaphthalen-2-amine was optically resolved, using CHIRALPAK AD-H (20 mm×250 mm) (hexane/isopropanol/diethylamine=85/15/0.1) to obtain 237 mg of (7R*)-7-[(dimethylamino)methyl]-5,6,7,8-tetrahydronaphthalen-2-amine, and 243 mg of (7S*)-7-[(dimethylamino)methyl]-5,6,7,8-tetrahydronaphthalen-2-amine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08436004B2
Source datasetuspto-grants-2013_05
ORD IDord-28550e0efdde4cc4b3ced0486792af9f
Source noteuspto-grants-2013_05