HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane isopropanol diethylamine → HCID 58289846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane isopropanol diethylamine | HCID 21973129 | — |
| Reactant | HCID 68653648 | HCID 68653648 | — |
| Product | HCID 58289846 | HCID 58289846 | — |
| Product | HCID 58289847 | HCID 58289847 | — |
Reaction Steps
N2,N2-dimethyl-1,2,3,4-tetrahydronaphthalene-2,6-diamine was optically resolved with CHIRALPAK AD-H (20 mm×250 mm) (hexane/isopropanol/diethylamine=80/20/0.1) to obtain 57.4 mg of (2S*)—N2,N2-dimethyl-1,2,3,4-tetrahydronaphthalene-2,6-diamine as a white solid, and 52.9 mg of (2R*)—N2,N2-dimethyl-1,2,3,4-tetrahydronaphthalene-2,6-diamine as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436004B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-b33813abbf9b4e1fb9ab75057695dad5 |
| Source note | uspto-grants-2013_05 |