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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2088824Generated: November 3, 2026

Thiophene → HCID 58625102, compound

https://huagongshe.com/reaction/2088824

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThiopheneHCID 8030—
ReactantHCID 58625080HCID 58625080—
CatalystPlatinumHCID 23939—
SolventMethanolHCID 887—
ProductHCID 58625102HCID 58625102—

Reaction Steps

A mixture of cyclohexyl-[3-(4-nitro-3-propylaminomethyl-phenoxy)-phenyl]-carbamic acid benzyl ester (0.00181 mol) in methanol (50 mL) was hydrogenated with 5% Pt/C (0.5 g) as a catalyst in the presence of thiophene solution (1 mL). After uptake of H2 (3 equiv), the catalyst was filtered off and the filtrate was evaporated to yield the title compound as a residue. which was used in subsequent reactions without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08436006B2
Source datasetuspto-grants-2013_05
ORD IDord-7f56cbba7f5047d39c2a06ea2c5b8389
Source noteuspto-grants-2013_05