HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldioxirane → 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldioxirane | HCID 115197 | — |
| Reactant | 8-Benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one | HCID 22499178 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one | HCID 57494231 | — |
Reaction Steps
To 8-benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one (300 mg) is added to a 0.1M solution of dimethyldioxirane in acetone (12.4 mL). After stirring at room temperature for 2 hours, the solvent is removed in vacuo to yield the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436017B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-bbe05355bdc6469bae6ea73f499531c6 |
| Source note | uspto-grants-2013_05 |