HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-chloro-1-methyl-4-nitro-1H-pyrazole → HCID 58464976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-chloro-1-methyl-4-nitro-1H-pyrazole | HCID 12344836 | — |
| Reactant | 1,4-Oxazepane | HCID 21873275 | — |
| Product | HCID 58464976 | HCID 58464976 | 52% |
Reaction Steps
Reaction of 5-chloro-1-methyl-4-nitro-1H-pyrazole and 1,4-oxazepane gave 4-(1-methyl-4-nitro-1H-pyrazol-5-yl)-1,4-oxazepane as a yellow oil (72 mg, 52%). 1H NMR (400 MHz, CDCl3) δ 8.03 (s, 1H), 3.94 (t, J=5.6 Hz, 2H), 3.88-3.84 (m, 2H), 3.80 (s, 3H), 3.40-3.35 (m, 4H), 2.07-1.99 (m, 2H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436001B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-227fd738a94b4ab084779ad5c6d90bdf |
| Source note | uspto-grants-2013_05 |