HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cis-2-boc-hexahydropyrrolo[3,4-C]pyrrole → HCID 58464847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cis-2-boc-hexahydropyrrolo[3,4-C]pyrrole | HCID 1514452 | — |
| Reactant | 5-chloro-1-methyl-4-nitro-1H-pyrazole | HCID 12344836 | — |
| Product | HCID 58464847 | HCID 58464847 | 86% |
Reaction Steps
Reaction of 5-chloro-1-methyl-4-nitro-1H-pyrazole and (3aR,6aS)-tert-butyl hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate gave (3aR,6aS)-tert-butyl 5-(1-methyl-4-nitro-1H-pyrazol-5-yl)hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate as a yellow oil (0.36 g, 86%). 1H NMR (400 MHz, CDCl3) δ 8.05 (s, 1H), 3.75 (s, 3H), 3.73-3.55 (m, 4H), 3.42-3.33 (m, 2H), 3.17-3.04 (m, 4H), 1.48 (s, 9H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436001B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-c4a7c6b8006748f0b285ab0da8d18253 |
| Source note | uspto-grants-2013_05 |