HCID 66958491, compound → HCID 66958404, compound

Participants

Reaction Steps

The product from step (ii) (12 g) was dissolved in dry THF (250 mL), 1% Pt/C catalyst (3 g) was added and the reaction mixture hydrogenated (H2 pressure: 3 bar) for 72 h at rt. The product was filtered through a glass fibre filter paper and purified via neutral Aluminum oxide column eluting with 4% MeOH in DCM and further purified via RPHPLC to give subtitle compound, yield 1.3 g.

Provenance & Evidence