m-Chloroperbenzoic acid → HCID 22478983, compound

Participants

Reaction Conditions

Reaction Steps

The product from step (iv) (0.9 g) was dissolved in DCM (25 mL) and cooled to 5° C. 3-Chloroperoxybenzoic acid (0.203 g) was added and the reaction was allowed to warm to rt. The reaction mixture was stirred for 2 h, more 3-chloroperoxybenzoic acid (0.30 g) was added and the reaction mixture stirred for a further 2 h. The reaction mixture was poured into saturated sodium bisulfate solution, extracted with DCM, dried, filtered and evaporated to give the subtitle (0.9 g).

Provenance & Evidence