HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → HCID 86232752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 66924472 | HCID 66924472 | — |
| Catalyst | HCID 178419074 | HCID 178419074 | — |
| Product | HCID 86232752 | HCID 86232752 | — |
Reaction Steps
By a similar operation as in Reference Example 15 and using [5-(2-fluorophenyl)-4-methyl-1H-pyrrol-3-yl]methanol (1.17 g), tetra-n-propylammonium perruthenate (101 mg), N-methylmorpholine N-oxide (1.01 g) and molecular sieves 4A powder (572 mg), the title compound was obtained as pale-pink crystals (yield 0.67 g, 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436187B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-d5e15efd9083476784554c855df1802e |
| Source note | uspto-grants-2013_05 |