HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 66777966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethylhydrazine | HCID 29062 | — |
| Reactant | 1-(4-(Trifluoromethoxy)phenyl)ethan-1-one | HCID 522821 | — |
| Product | HCID 66777966 | HCID 66777966 | 92% |
Reaction Steps
Using 1-[4-(trifluoromethoxy)phenyl]ethanone (13.0 g), sodium hydride (60%, oily, 2.8 g), diethyl oxalate (8.7 mL) and ethylhydrazine (4.2 g) and in the same manner as in Example 56(1), the title object compound (19.4 g, 92%) was obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08436043B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-336f484db15743978f6370fbdd65a7bf |
| Source note | uspto-grants-2013_05 |