HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 57939190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57939210 | HCID 57939210 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57939190 | HCID 57939190 | 99.4% |
Reaction Steps
300 μL of 1 N sodium hydroxide solution (300 μmol) are added portionwise to 48 mg of 25 (157 μmol) in methanol (2 mL). The solution is refluxed for 1 hour 30 minutes. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 45 mg of a pale yellow oil are obtained, i.e. a yield of 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440591B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-06610782bf1341f886970ef8621cd8df |
| Source note | uspto-grants-2013_05 |