HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 3,4-Dihydro-2H-1-benzopyran-4-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Chroman-4-one O-methyl-oxime | HCID 54035320 | — |
| Edukt | (4E)-N-Methoxy-6-methyl-3,4-dihydro-2H-1-benzopyran-4-imine | HCID 86605441 | — |
| Produkt | 3,4-Dihydro-2H-1-benzopyran-4-amine | HCID 4961957 | — |
Reaktionsschritte
The title compound was prepared using the procedure as described in Example 7B, substituting the product of Example 16A for the product of Example 7A. 1H NMR (300 MHz, DMSO-d6) δ ppm 7.32 (dd, J 1.0 and 7.5 Hz, 1H), 7.05 (m, 1H), 6.81 (m, 1H), 6.70 (dd, J 1.0 and 7.5 Hz, 1H), 4.27-4.08 (m, 2H), 3.83 (t, J 6.0 Hz, 1H), 2.03-1.66 (m, 4H). MS (DCI/NH3) m/e 150 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08440691B2 |
| Quelldatensatz | uspto-grants-2013_05 |
| ORD ID | ord-1ff257f7d91d406fbd18fa2cdfbbf7ad |
| Quellennotiz | uspto-grants-2013_05 |