HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 5-Amino-adamantane-2-thione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 58192775 | HCID 58192775 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 5-Amino-adamantane-2-thione | HCID 51038909 | 110.3% |
Reaction Steps
To 10B (30 mg, 0.10 mmol) was added HBr (33% in HOAc) 2 mL and the mixture was stirred at rt for 1 h. Ether (10 mL×2) was added and the resulting precipitate was collected and dried under vacuum to give the title compound as hydrogen bromide salts (10) (20 mg). LC-MS (ESR): m/z=182 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08440720B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-7676ff99902746c39bda638a3b69918a |
| Source note | uspto-grants-2013_05 |