Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Tetradecyl Sulfate | HCID 23665772 | — |
| Product | Isostearyl Alcohol EX | HCID 62825 | 21.9% |
Reaction Steps
The reaction mixture was emulsified as follows: 300 g polycarbodiimide solution as prepared above was heated to 65° C. and added to a hot aqueous solution of Ethoquad™ C-12 (2% on solids), Tergitol 15S30 (3% on solids) and Tergitol™ TMN-6 (5.4% solids). 199 g water was added. The mixture was emulsified with 2 stage lab Manton-Gaulin at 220/20 bar (2 passes). The solvent was stripped off with a Büchi evaporator, using water jet vacuum. A stable, milky dispersion of 21.9% solids was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08440779B2 |
|---|
| Source dataset | uspto-grants-2013_05 |
|---|
| ORD ID | ord-63bbf96a8d834fe8a9d77d793d7a2a41 |
|---|
| Source note | uspto-grants-2013_05 |
|---|
