HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Methylsulfonyl)piperazine → HCID 44545154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Methylsulfonyl)piperazine | HCID 709161 | — |
| Reactant | HCID 66909826 | HCID 66909826 | — |
| Product | HCID 44545154 | HCID 44545154 | — |
Reaction Steps
3-(2-(2-(Tert-butoxycarbonylamino)pyrimidin-5-yl)-6-morpholino-9H-purin-9-yl)propanoic acid (50 mg) was reacted with 1-(methylsulfonyl)piperazine via General Procedure F followed by Boc deprotection via General Procedure E to give 33.8 mg 112 as white solid following reverse phase purification. MS (Q1) 517.2 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445487B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-02536a162c0b41d6ae737261c13a0d73 |
| Source note | uspto-grants-2013_05 |