HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methylpiperidine-4-carboxamide → HCID 44545387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methylpiperidine-4-carboxamide | HCID 2760460 | — |
| Reactant | HCID 58015218 | HCID 58015218 | — |
| Product | HCID 44545387 | HCID 44545387 | — |
Reaction Steps
2-(2-(2-(Tert-butoxycarbonylamino)pyrimidin-5-yl)-6-morpholino-9H-purin-9-yl)acetic acid (35 mg) was reacted with N-methylpiperidine-4-carboxamide via General Procedure F followed by Boc deprotection via General Procedure E and purified via reverse phase HPLC to give 10.3 mg 122 as a white solid. MS (Q1) 481.2 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445487B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-453a08a1857845cba03d5bb5700965d3 |
| Source note | uspto-grants-2013_05 |