HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 59178968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 59178931 | HCID 59178931 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59178968 | HCID 59178968 | — |
Reaction Steps
A solution of tert-Butyl 1′-(4-formylphenyl)-4,4′-bipiperidine-1-carboxylate (72 mg; 0.193 mmol) in EtOH (1 mL) was treated with NaBH4 (8 mg; 0.213 mmol). The solution was stirred at ambient temperature for 1 hr. The reaction was partitioned between iPrOAc and water. The organic was dried over magnesium sulfate, filtered and evaporated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445499B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-9d4bb0b6039e40ebbad0941fb43e5a39 |
| Source note | uspto-grants-2013_05 |