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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2093701Generated: October 31, 2026

Benzamide → HCID 178484329, compound

https://huagongshe.com/reaction/2093701

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzamideHCID 2331—
ReactantDimethylformamide dimethyl acetalHCID 78373—
ProductHCID 178484329HCID 178484329—

Reaction Steps

A solution of benzamide (1-135) in DMF-DMA was stirred for 3 h at 110° C., then cooled to rt. The solid was collected by filtration, the filter cake washed with PE and air dried to give the desired (E)-N-((dimethylamino)methylene)benzamide (compound II-135).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08445503B2
Source datasetuspto-grants-2013_05
ORD IDord-3bbf2f0d31874c6f86fabf84399c3a6e
Source noteuspto-grants-2013_05