HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67167138, compound → HCID 58257116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67167138 | HCID 67167138 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58257116 | HCID 58257116 | — |
Reaction Steps
The 5-(2,5-dimethyl-4-nitrophenyl)oxazole obtained in the last step was dissolved in methanol (10 mL). To the solution was added Pd/C (10%). The reaction mixture was degassed and purged with H2 for several times and then stirred under 1 atm. hydrogen gas overnight. The mixture was filtered and concentrated to afford 2,5-dimethyl-4-(oxazol-5-yl)aniline as a white solid. ESMS m/z 189 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445505B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-2b28c50b7b594702a6eb50371944b473 |
| Source note | uspto-grants-2013_05 |