Acetic-formic anhydride → HCID 86650180, compound

HRID 2094066Notes

Reaction equation

HRID 2094066 reaction equation
[NH:1]1[CH2:6][CH2:5][CH:4]([NH:7][C:8]([C:10]2[C:14]3[N:15]=[CH:16][N:17]=[C:18]([C:19]4[C:27]5[O:26][CH2:25][O:24][C:23]=5[CH:22]=[CH:21][C:20]=4[O:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:13]=3[NH:12][CH:11]=2)=[O:9])[CH2:3][CH2:2]1.[CH:33](OC(=O)C)=[O:34]>>[CH:33]([N:1]1[CH2:6][CH2:5][CH:4]([NH:7][C:8]([C:10]2[C:14]3[N:15]=[CH:16][N:17]=[C:18]([C:19]4[C:27]5[O:26][CH2:25][O:24][C:23]=5[CH:22]=[CH:21][C:20]=4[O:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:13]=3[NH:12][CH:11]=2)=[O:9])[CH2:3][CH2:2]1)=[O:34]

Participants

3

Reactant 2

HCID 75269Acetic-formic anhydrideHCID 66867038HCID 66867038, compound

Product 1

HCID 86650180HCID 86650180, compound

Procedure

Starting from 4-(5-butoxy-benzo[1,3]dioxol-4-yl)-5H-pyrrolo[3,2-d]pyrimidine-7-carboxylic acid piperidin-4-ylamide (example A179) and acetic formic anhydride the title compound was obtained as colorless solid.

Sources & evidence

ORD record
ord-6330ca09ccb04de4934b61a4d1a613de
Source dataset
uspto-grants-2013_05
Patent number
US08445501B2

Reaction notes

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