Aluminium lithium hydride → HCID 178430916, compound

Participants

Reaction Steps

The titled compound was prepared according to general Method B using 4-chloro-N-(2-(hydrazinecarbonyl)-5-chloropyridin-3-yl)-3-(trifluoromethyl)benzenesulfonamide and 3-amino-4-hydroxymethylpyrazole ((MS, 409 [M+H]+, which was generated in situ by reduction of ethyl 3-amino-1H-pyrazole-4-carboxylate using LAH in THF): 1H NMR (400 MHz, CDCl3) δ 8.28 (s, 1H), 8.16 (d, 1H), 8.13 (d, 1H), 7.97 (d, 1H), 7.94 (dd, 1H), 7.56 (d, 1H), 7.42 (d. 1H), 1.65 (s, 3H). MS (ES) [M+H]+ expected 518.0. found 518.0.

Provenance & Evidence