HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 44546612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 44548798 | HCID 44548798 | — |
| Product | HCID 44546612 | HCID 44546612 | — |
Reaction Steps
By reacting 1-(4-(4-(8-oxa-3-azabicyclo[3.2.1]octan-3-yl)-6-(4-oxopiperidin-1-yl)-1,3,5-triazin-2-yl)phenyl)-3-(pyridin-4-yl)urea.TFA (40 mg) and 1-methylpiperazine (0.050 mL) and following the procedure as outlined in example 118, the titled compound was isolated after HPLC purification as its tri-TFA salt; MS (ES+) 585.9 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445486B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-60447b2e16a74920aa8200774d324b2c |
| Source note | uspto-grants-2013_05 |