Sodium Methoxide → HCID 58103524, compound

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Reaction Steps

To the product of Step A (6.645 g, 17.3 mol) in MeOH (60 mL) was added sodiummethoxide (5.92 mL, 25.9 mmol, 25 wt %) at rt. After 20 min the reaction was concentrated and then diluted with EtOAc and washed with aq HCl (2M) and then water providing the unpurified title compound (RE-2) which was used directly in Reference Example 3. HPLC/MS: 353.0 (M+1); Rt=2.68 min.

Provenance & Evidence