Benzyl Bromide → HCID 25205356, compound

Participants

Reaction Steps

Prepared as in example 5-10 from (2,4-dimethoxyphenyl)methanamine, methyl 4-(chlorosulfonyl)benzoate (Example 5-10c) and benzyl bromide. MS (M−H, 440.10); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.50(s, 63H), 3.66(s, 3H), 4.20(s, 2H), 4.34(s, 2H), 6.29(s, 1H), 6.33(d, J=8.0 Hz, 1H), 6.91(d, J=8.8 Hz, 1H), 7.12-7.23 (m, 5H), 7.80(d, J=8.0 Hz, 2H), 8.01 (d, J=8.4 Hz, 2H), 13.49(s, 1H).

Provenance & Evidence