Benzyl Bromide → HCID 57422337, compound

Participants

Reaction Steps

Prepared as in example 5-10 from (2,4,6-trimethoxyphenyl)methanamine, methyl 4-(chlorosulfonyl)benzoate (Example 5-10c) and benzyl bromide. MS (M−H, 470.10); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.45(s, 6H), 3.69(s, 3H), 4.26(s, 2H), 4.28(s, 2H), 5.98(s, 2H), 7.11-7.26(m, 5H), 7.82(d, J=8.0 Hz, 2H), 8.07(d, J=8 Hz, 2H), 13.49(s, 1H). Elemental analysis (found, %): C, 61.05; H, 5.49; N, 2.98; (calculated, %): C, 61.13; H, 5.34 and N, 2.97.

Provenance & Evidence