HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 25205188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | Methyl 4-(Chlorosulfonyl)benzoate | HCID 4738388 | — |
| Product | HCID 25205188 | HCID 25205188 | — |
Reaction Steps
Prepared as in example 5-10 from aniline, methyl 4-(chlorosulfonyl)benzoate (Example 5-10c) and 1-(chloromethyl)-4-methoxybenzene. MS (M−H, 396.1); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.66(s, 3H), 4.73(s, 2H), 6.78(d, J=8.4 Hz, 2H), 7.00(d, J=7.6 Hz, 2H), 7.12(d, J=8.0 Hz, 2H), 7.24(d, J=8.0 Hz, 2H), 8.11(d, J=8.4 Hz, 2H), 13.49(s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445692B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-865619bcf0184fa08df81e470dec0af1 |
| Source note | uspto-grants-2013_05 |