HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Aminomethyl)cyclohexanecarboxylic acid → HCID 25205186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Aminomethyl)cyclohexanecarboxylic acid | HCID 5526 | — |
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Product | HCID 25205186 | HCID 25205186 | — |
Reaction Steps
Prepared as in example 5-11 from benzenesulfonyl chloride, 4-(aminomethyl)-cyclohexanecarboxylic acid and 1-(bromomethyl)-4-fluorobenzene. MS (M+H, 406); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 0.77 (m, 2H), 0.94 (m, 2H), 0.98 (m, 2H), 1.50 (m, 2H0, 1.75 (m, 2H), 1.77 (m, 1H), 2.80 (d, 2H), 4.28 (s, 2H), 7.20 (m, 2H), 7.38(m, 2H), 7.62(m, 2H), 7.70(m, 1H), 7.88(m, 2H), 11.93(br, s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445692B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-e67db74e873f49a89a967b59e9881895 |
| Source note | uspto-grants-2013_05 |