HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → Triphenyl(4-phenylbutyl)phosphonium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | (4-Iodobutyl)benzene | HCID 12709818 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Triphenyl(4-phenylbutyl)phosphonium iodide | HCID 86642679 | 62.2% |
Reaction Steps
A solution of (4-iodobutyl)benzene (1.04 g, 4.0 mmol) and Ph3P (1.05 g, 4.0 mmol) in CH3CN (20 mL) was stirred for 48 h and then washed with hexane. The solvent was removed to afford triphenyl(4-phenylbutyl)phosphonium iodide (1.30 g, 62%) as a white foam, which was used in the following step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08445684B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-af5a14f92e494fdf9fcb37390f9ec907 |
| Source note | uspto-grants-2013_05 |