HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2095861Generated: November 2, 2026
Ethyl cyanoacetate → HCID 17026974, compound
https://huagongshe.com/reaction/2095861
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | 4-Fluoro-m-toluidine | HCID 67981 | — |
| Product | HCID 17026974 | HCID 17026974 | 95% |
Reaction Steps
A mixture of 4-fluoro-3-methylaniline (2.50 g, 20.0 mmol) and ethyl cyanoacetate (2.70 g, 24.0 mmol) was stirred at 180° C. for 14 hr. After cooling to room temperature, the obtained solid was washed with hexane and collected by filtration to give the title compound (3.60 g, 95%) as a brownish-red solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08445509B2 |
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| Source dataset | uspto-grants-2013_05 |
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| ORD ID | ord-fdf1e57d46ff42c5ab4dfe71190274fa |
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| Source note | uspto-grants-2013_05 |
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