3-Methyl-isothiazole → HCID 59556170, compound

HRID 2096222Notes

Reaction equation

HRID 2096222 reaction equation
[CH3:1][C:2]1[CH:6]=[CH:5][S:4][N:3]=1.[O:7]1[C:11]2([CH2:16][CH2:15][C:14](=[O:17])[CH2:13][CH2:12]2)[O:10][CH2:9][CH2:8]1>CCOCC>[CH3:1][C:2]1[CH:6]=[C:5]([C:14]2([OH:17])[CH2:15][CH2:16][C:11]3([O:10][CH2:9][CH2:8][O:7]3)[CH2:12][CH2:13]2)[S:4][N:3]=1

Participants

4

Reactant 2

HCID 127473-Methyl-isothiazoleHCID 5674151,4-Dioxaspiro[4.5]decan-8-one

Product 1

HCID 59556170HCID 59556170, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The title compound was prepared as a white solid from 3-methyl-isothiazole (Focus Synthesis) and 1,4-dioxa-spiro[4.5]decan-8-one in ether using the procedure described in Step A of Example 33.

Sources & evidence

ORD record
ord-402574f6c0994123bbcd9079c0ecf76d
Source dataset
uspto-grants-2013_05
Patent number
US08450304B2

Reaction notes

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