HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetramethylammonium fluoride → HCID 66697236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetramethylammonium fluoride | HCID 67803 | — |
| Reactant | (Trifluoromethyl)trimethylsilane | HCID 552549 | — |
| Reactant | HCID 66697356 | HCID 66697356 | — |
| Product | HCID 66697236 | HCID 66697236 | — |
Reaction Steps
In analogy to Example 1, step 3, 8-[2-(4-bromo-2-chloro-phenyl)-propionyl]-4-methyl-4H-benzo[1,4]oxazin-3-one was reacted with (trifluoromethyl)trimethylsilane and tetramethylammonium fluoride to give the title compound as a colorless foam. MS (m/e, ISP neg. ion)=476 [M−H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450313B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-4624cbafd81242ef9fcd748c8cb4bfa7 |
| Source note | uspto-grants-2013_05 |