7-Phenylheptan-1-amine → 3-(7-Phenylheptylamino)-4-(pyridin-4-yl-amino)-cyclobut-3-ene-1,2-dione

HRID 2097329Notes

Reaction equation

HRID 2097329 reaction equation
C(O[C:4]1[C:5](=[O:16])[C:6](=[O:15])[C:7]=1[NH:8][C:9]1[CH:14]=[CH:13][N:12]=[CH:11][CH:10]=1)C.[C:17]1([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][NH2:30])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:17]1([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][NH:30][C:4]2[C:5](=[O:16])[C:6](=[O:15])[C:7]=2[NH:8][C:9]2[CH:10]=[CH:11][N:12]=[CH:13][CH:14]=2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 64319907-Phenylheptan-1-amineHCID 106803193-Ethoxy-4-(pyridin-4-ylamino)cyclobut-3-ene-1,2-dione

Product 1

HCID 115886123-(7-Phenylheptylamino)-4-(pyridin-4-yl-amino)-cyclobut-3-ene-1,2-dioneYield 59%

Procedure

The title compound was prepared according to the procedure described in example 1B starting from 3-ethoxy-4-(pyridin-4-yl-amino)-3-cyclobutene-1,2-dione prepared according to example 7A and 7-phenylheptylamine.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-52c67fa5365540a6bbe6da77fddf9907
Source dataset
uspto-grants-2013_05
Patent number
US08450348B2

Reaction notes

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