HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 59174604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 59174424 | HCID 59174424 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59174604 | HCID 59174604 | — |
Reaction Steps
The title compound was prepared by treating the product of Example 85 with acetic anhydride and pyridine in CH2Cl2 at rt for 1 hr, followed by washing with 1N HCl, then with aqueous NaHCO3, drying over Na2SO4 and removal of solvents in vacuo. MS m/z: 449.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450335B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-84b8cf9f93e346b7a0179775fbf3fdde |
| Source note | uspto-grants-2013_05 |