HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzofuran-2-sulfonyl chloride → N-[2-(benzylthio)-5-cyanophenyl]-1-benzofuran-2-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| Reactant | HCID 43518344 | HCID 43518344 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-[2-(benzylthio)-5-cyanophenyl]-1-benzofuran-2-sulfonamide | HCID 67972124 | 65% |
Reaction Steps
Following General Procedure B, the title compound (419 mg, 65%) was prepared from 3-amino-4-(benzylthio)benzonitrile (370 mg, 1.54 mmol) and benzofuran-2-sulfonyl chloride (333 mg, 1.54 mmol) in pyridine (3 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450367B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-6f8eb1f5b70043dea25073611e6d70c2 |
| Source note | uspto-grants-2013_05 |