HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-bromo-3-(4H-1,2,4-triazol-3-yl)thiophen-2-amine → HCID 56665247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-bromo-3-(4H-1,2,4-triazol-3-yl)thiophen-2-amine | HCID 59636686 | — |
| Reactant | HCID 68785094 | HCID 68785094 | — |
| Product | HCID 56665247 | HCID 56665247 | — |
Reaction Steps
The title compound was prepared from 2-(2-oxo-6-(trifluoromethoxy)quinolin-1(2H)-yl)acetic acid (40 mg, 0.14 mmol) and 4-bromo-3-(1H-1,2,4-triazol-5-yl)thiophen-2-amine (28 mg, 0.11 mmol) according to protocol A. Retention time (min)=6.06, method [7], MS (ESI) 514.0 (M+H); 1H NMR (300 MHz, CD3C1) δ 7.85 (d, J=9.35 Hz, 1H), 7.73 (s, 1H), 7.50 (s, 1H), 7.44-7.41 (m, 1H), 7.35-7.33 (m, 1H), 6.97 (d, J=9.9 Hz, 1H), 6.95 (s, 1H), 5.31 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450363B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-3a6daa7cc406453880230bb4077e1182 |
| Source note | uspto-grants-2013_05 |